The synthesis of [2-13C]2-nitropropane at room temperature and at atmospheric pressure

2.50
Hdl Handle:
http://hdl.handle.net/10029/256978
Title:
The synthesis of [2-13C]2-nitropropane at room temperature and at atmospheric pressure
Authors:
Jacquemijns M; Zomer G
Other Titles:
De synthese van [2-13C]2-nitropropaan bij kamertemperatuur en atmosferische druk
Abstract:
In this report the synthesis of [2-13C]2-nitropropane at room temperature is described. [2-13C]Acetone was converted into the oxime with hydroxy hydrochloridelamine and sodium carbonate. Treatment with hypobromic acid resulted in 2-13C]2-bromo-2-nitropropane. Hydrogenation with sodium borohydride gave [2-13C]2-nitropropane in 14,3% overall yield.<br>
Publisher:
Rijksinstituut voor Volksgezondheid en Milieu RIVM
Issue Date:
31-Mar-1990
URI:
http://hdl.handle.net/10029/256978
Additional Links:
http://www.rivm.nl/bibliotheek/rapporten/328605004.html
Type:
Onderzoeksrapport
Language:
en
Sponsors:
RIVM
Appears in Collections:
RIVM official reports

Full metadata record

DC FieldValue Language
dc.contributor.authorJacquemijns M-
dc.contributor.authorZomer G-
dc.date.accessioned2012-12-12T14:55:37Z-
dc.date.available2012-12-12T14:55:37Z-
dc.date.issued1990-03-31-
dc.identifier328605004-
dc.identifier.urihttp://hdl.handle.net/10029/256978-
dc.description.abstractIn this report the synthesis of [2-13C]2-nitropropane at room temperature is described. [2-13C]Acetone was converted into the oxime with hydroxy hydrochloridelamine and sodium carbonate. Treatment with hypobromic acid resulted in 2-13C]2-bromo-2-nitropropane. Hydrogenation with sodium borohydride gave [2-13C]2-nitropropane in 14,3% overall yield.<br>en
dc.description.sponsorshipRIVM-
dc.format.extent15 p-
dc.language.isoen-
dc.publisherRijksinstituut voor Volksgezondheid en Milieu RIVM-
dc.relation.ispartofRIVM Rapport 328605004-
dc.relation.urlhttp://www.rivm.nl/bibliotheek/rapporten/328605004.html-
dc.subject20nl
dc.titleThe synthesis of [2-13C]2-nitropropane at room temperature and at atmospheric pressureen
dc.title.alternativeDe synthese van [2-13C]2-nitropropaan bij kamertemperatuur en atmosferische druknl
dc.typeOnderzoeksrapport-
dc.date.updated2012-12-12T14:55:38Z-
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