The synthesis of [2-13C]2-nitropropane at room temperature and at atmospheric pressure
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Open Access
Type
Report
Language
en
Date
1990-03-31
Research Projects
Organizational Units
Journal Issue
Title
The synthesis of [2-13C]2-nitropropane at room temperature and at atmospheric pressure
Translated Title
De synthese van [2-13C]2-nitropropaan bij kamertemperatuur en atmosferische druk
Published in
Abstract
In this report the synthesis of [2-13C]2-nitropropane at room temperature is described. [2-13C]Acetone was converted into the oxime with hydroxy hydrochloridelamine and sodium carbonate. Treatment with hypobromic acid resulted in 2-13C]2-bromo-2-nitropropane. Hydrogenation with sodium borohydride gave [2-13C]2-nitropropane in 14,3% overall yield.<br>
Description
Publisher
Rijksinstituut voor Volksgezondheid en Milieu RIVM
Sponsors
RIVM