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dc.contributor.authorJacquemijns M
dc.contributor.authorZomer G
dc.date.accessioned2012-12-12T14:55:37Z
dc.date.available2012-12-12T14:55:37Z
dc.date.issued1990-03-31
dc.identifier328605004
dc.identifier.urihttp://hdl.handle.net/10029/256978
dc.description.abstractIn this report the synthesis of [2-13C]2-nitropropane at room temperature is described. [2-13C]Acetone was converted into the oxime with hydroxy hydrochloridelamine and sodium carbonate. Treatment with hypobromic acid resulted in 2-13C]2-bromo-2-nitropropane. Hydrogenation with sodium borohydride gave [2-13C]2-nitropropane in 14,3% overall yield.<br>
dc.description.sponsorshipRIVM
dc.format.extent15 p
dc.language.isoen
dc.publisherRijksinstituut voor Volksgezondheid en Milieu RIVM
dc.relation.ispartofRIVM Rapport 328605004
dc.relation.urlhttp://www.rivm.nl/bibliotheek/rapporten/328605004.html
dc.subject20nl
dc.titleThe synthesis of [2-13C]2-nitropropane at room temperature and at atmospheric pressureen
dc.title.alternativeDe synthese van [2-13C]2-nitropropaan bij kamertemperatuur en atmosferische druknl
dc.typeReport
dc.date.updated2012-12-12T14:55:38Z
html.description.abstractIn this report the synthesis of [2-13C]2-nitropropane at room temperature is described. [2-13C]Acetone was converted into the oxime with hydroxy hydrochloridelamine and sodium carbonate. Treatment with hypobromic acid resulted in 2-13C]2-bromo-2-nitropropane. Hydrogenation with sodium borohydride gave [2-13C]2-nitropropane in 14,3% overall yield.&lt;br&gt;


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