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    Prestatiekenmerken van de bepaling van formaldehyde en 8-hydroxychinolinesulfaat

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    Authors
    Cleven RFMJ
    Graaf M de
    Type
    Report
    Language
    nl
    
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    Title
    Prestatiekenmerken van de bepaling van formaldehyde en 8-hydroxychinolinesulfaat
    Translated Title
    Performance characteristics of the determination of formaldehyde and 8-hydroxychinolinesulphate
    Publiekssamenvatting
    Een aantal prestatiekenmerken voor de bepaling van een tweetal componenten waarvan de gehaltes regelmatig worden bepaald in voornamelijk sera en vaccins, is nader vastgelegd. Het betreft juistheid, precisie en nauwkeurigheid, de lineariteit van de kalibratiecurven, aantoonbaarheidsgrens, en matrix-effecten op precisie en nauwkeurigheid van de fotometrische bepalingen van formaldehyde en 8-hydroxy-chinolinesulfaat. De nauwkeurigheid blijkt voor formaldehyde beter dan 5%, en voor 8-hydroxychinolinesulfaat beter dan 3% over vrijwel de gehele meetbereiken van de methodes. De aantoonbaarheidsgrenzen bedragen 5 en 0,5 mumol/l voor respectievelijk formaldehyde en 8-hydroxychinolinesulfaat.
    Performance characteristics of the determinations of two components that are frequently analysed in sera and vaccines, have been established. It concerns trueness, precision and accuracy, the linearity of the calibration curves, the limit of detection and matrix effects on precision and accuracy of the photometric determinations of formaldehyde and 8-hydroxychinoline-sulphate. It appears that for formaldehyde the accuracy is better than 5%, and for 8-hydroxychinoline-sulphate the accuracy is better than 3% over nearly the whole concentration ranges covered by the methods. The limits of detection of the methods are 5 and 0.5 mumol/l for formaldehyde and 8-hydroxychinolinesulphate respectively, for the undiluted samples.
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    RIVM
    URI
    http://hdl.handle.net/10029/257063
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